1. | Course Title | Methods and Instrumentation for Quantitative Analysis of Materials | |||||||||||
2. | Code | 4ФЕИТ08011 | |||||||||||
3. | Study program | 15-MMK | |||||||||||
4. | Organizer of the study program (unit, institute, department) | Faculty of Electrical Engineering and Information Technologies | |||||||||||
5. | Degree (first, second, third cycle) | Second cycle | |||||||||||
6. | Academic year/semester | I/1 | 7. | Number of ECTS credits | 6.00 | ||||||||
8. | Lecturer | Dr Lihnida Stojanovska-Georgievska | |||||||||||
9. | Course Prerequisites | ||||||||||||
10. | Course Goals (acquired competencies):
Introduction to a range of modern analytical techniques used in research laboratories to analyse the matter. Students are expected to enhance their knowledge on the theoretical aspects, design and operation of a number of instruments used in the analysis of physical quantities. Ultimately, students will improve their analytical thinking by recognizing and understanding the advantages and disadvantages of the instrumental methods to be used depending on the material under investigation. |
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11. | Course Syllabus:
Theoretical aspects on physical methods for material analysis: separation, qualitative and quantitative optical spectroscopic techniques, mass spectrometry, electroanalytical techniques and surface analysis, chromatography, electrochemistry. Introduction to the principle of operation and design of instruments, sample preparation for organic and inorganic samples, quantitative analysis, sensitivity and limit of detection used in measurements of physical quantities of substrates, thin films, liquids, biological materials, food and artificial materials. Testing methods in trace analysis and residues detection, contamination detection and identification of unknown substances. Principles of traceability, detectability and reliability. Advanced analytical instrumentation or a combination of techniques, testing protocols according to standard methodologies (ISO, EN, BS, ASTM, DIN, etc.) in order to develop tailored analytical methods and to perform method validation for specific testing applications. The emphasis for the program is on measurement methods in general physics, technology, electronics, environmental physics, food safety and related industrial applications. |
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12. | Learning methods:
lectures, electronic attendance, teamwork, seminar works, presentations |
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13. | Total number of course hours | 180 | |||||||||||
14. | Distribution of course hours | 3 + 3 | |||||||||||
15. | Forms of teaching | 15.1 | Lectures-theoretical teaching | 45 hours | |||||||||
15.2 | Exercises (laboratory, practice classes), seminars, teamwork | 45 hours | |||||||||||
16. | Other course activities | 16.1 | Projects, seminar papers | 30 hours | |||||||||
16.2 | Individual tasks | 30 hours | |||||||||||
16.3 | Homework and self-learning | 30 hours | |||||||||||
17. | Grading | ||||||||||||
17.1 | Exams | 30 points | |||||||||||
17.2 | Seminar work/project (presentation: written and oral) | 50 points | |||||||||||
17.3. | Activity and participation | 20 points | |||||||||||
17.4. | Final exam | points | |||||||||||
18. | Grading criteria (points) | up to 50 points | 5 (five) (F) | ||||||||||
from 51 to 60 points | 6 (six) (E) | ||||||||||||
from 61 to 70 points | 7 (seven) (D) | ||||||||||||
from 71 to 80 points | 8 (eight) (C) | ||||||||||||
from 81 to 90 points | 9 (nine) (B) | ||||||||||||
from 91 to 100 points | 10 (ten) (A) | ||||||||||||
19. | Conditions for acquiring teacher’s signature and for taking final exam | 60% success from all pre-exam activities | |||||||||||
20. | Forms of assessment | Preparation and presentation of a project assignment | |||||||||||
21. | Language | Macedonian and English | |||||||||||
22. | Method of monitoring of teaching quality | Selfevaluation | |||||||||||
23. | Literature | ||||||||||||
23.1. | Required Literature | ||||||||||||
No. | Author | Title | Publisher | Year | |||||||||
1. | Alice Groysman | Modern Analytical Techniques: Methods and Separation | Alexis Press LLC | 2019 | |||||||||
2. | Kelly Morrison | Characterisation Methods in Solid State and Materials Science | IOP Publishing | 2019 |