Methods and Instrumentation for Quantitative Analysis of Materials

Објавено: July 11, 2023
1. Course Title Methods and Instrumentation for Quantitative Analysis of Materials
2. Code 4ФЕИТ08011
3. Study program 15-MMK
4. Organizer of the study program (unit, institute, department) Faculty of Electrical Engineering and Information Technologies
5. Degree (first, second, third cycle) Second cycle
6. Academic year/semester I/1   7.    Number of ECTS credits 6.00
8. Lecturer Dr Lihnida Stojanovska-Georgievska
9. Course Prerequisites
10. Course Goals (acquired competencies):

Introduction to a range of modern analytical techniques used in research laboratories to analyse the matter. Students are expected to enhance their knowledge on the theoretical aspects, design and operation of a number of instruments used in the analysis of physical quantities. Ultimately, students will improve their analytical thinking by recognizing and understanding the advantages and disadvantages of the instrumental methods to be used depending on the material under investigation.

11. Course Syllabus:

Theoretical aspects on physical methods for material analysis: separation, qualitative and quantitative optical spectroscopic techniques, mass spectrometry, electroanalytical techniques and surface analysis, chromatography, electrochemistry. Introduction to the principle of operation and design of instruments, sample preparation for organic and inorganic samples, quantitative analysis, sensitivity and limit of detection used in measurements of physical quantities of substrates, thin films, liquids, biological materials, food and artificial materials. Testing methods in trace analysis and residues detection, contamination detection and identification of unknown substances. Principles of traceability, detectability and reliability. Advanced analytical instrumentation or a combination of techniques, testing protocols according to standard methodologies (ISO, EN, BS, ASTM, DIN, etc.) in order to develop tailored analytical methods and to perform method validation for specific testing applications. The emphasis for the program is on measurement methods in general physics, technology, electronics, environmental physics, food safety and related industrial applications.

12. Learning methods:

lectures, electronic attendance, teamwork, seminar works, presentations

13. Total number of course hours 180
14. Distribution of course hours 3 + 3
15. Forms of teaching 15.1 Lectures-theoretical teaching 45 hours
15.2 Exercises (laboratory, practice classes), seminars, teamwork 45 hours
16. Other course activities 16.1 Projects, seminar papers 30 hours
16.2 Individual tasks 30 hours
16.3 Homework and self-learning 30 hours
17. Grading
17.1 Exams 30 points
17.2 Seminar work/project (presentation: written and oral) 50 points
17.3. Activity and participation 20 points
17.4. Final exam  points
18. Grading criteria (points) up to 50 points     5 (five) (F)
from 51 to 60 points     6 (six) (E)
from 61 to 70 points     7 (seven) (D)
from 71 to 80 points     8 (eight) (C)
from 81 to 90 points     9 (nine) (B)
from 91 to 100 points   10 (ten) (A)
19. Conditions for acquiring teacher’s signature and for taking final exam 60% success from all pre-exam activities
20. Forms of assessment Preparation and presentation of a project assignment
21. Language Macedonian and English
22. Method of monitoring of teaching quality Selfevaluation
23. Literature
23.1.       Required Literature
No. Author Title Publisher Year
1. Alice Groysman Modern Analytical Techniques: Methods and Separation Alexis Press LLC 2019
2. Kelly Morrison Characterisation Methods in Solid State and Materials Science IOP Publishing 2019